This standard is issued under the fixed designation A ; the number immediately following 1 These practices are under the jurisdiction of ASTM Committee A01 on Steel, containing welds should be cut so that no more than 13 mm (1⁄2. Fast, high-quality ASTM A intergranular corrosion testing run by corrosion experts. ASTM has standardized the test procedure and the specifications are detailed in ASTM A standard (ASTM, ) and ASTM G standard (ASTM.
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The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion. For example, many low-carbon and stabilized stainless steels e. G2MT Labs is one of the few labs to offer all five ASTM A corrosion testing practices, as well as the expertise to help you determine which tests to use, what to do if a test fails, and other corrosion consulting as needed.
In many cases we can reduce that to as little as 24 hours more than the required testing aatm if you need fast results. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described asfm each testing practice. Practice B, also known as the Streicher test, uses weight loss analysis to provide a quantitative measure of the materials aztm.
Resistance to Intergranular Corrosion of Austenitic Stainless Steels
Link to Active This link will always route to the current Active version of the standard. The test is generally performed for acceptance of materials, but not sufficient for rejection of materials. It depends on which Practice is selected, but typically ranges from to days for different tests. Based on your materials, application, and requirements, the other 4 methods provide specific focuses.
The inch-pound equivalents are in parentheses and may be approximate. Some specific hazards statements are given in The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.
The weight loss is calculated after each step, and reveals if the sample has been properly heat-treated. The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:.
The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid.
If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed. Share on Tumblr Print. A recent publication on intergranular corrosion. Like what you saw?
These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared.
In everyday applications, corrosion varies by materials and solutions. Duplicate samples from both sides of a sheet sample ast, evaluated to determine if carburization results in intergranular attack.
This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. If you are not sure, please contact us for assistance. How do you select the right ASTM corrosion testing method for your material?
ASTM A Intergranular Corrosion Testing and Analysis
It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use astk application. Contact us now for pricing or a quote! Intergranular corrosion shows up as the dark black lines around the grain boundaries. This practice includes boiling the sample for 24 a2622-13 hours in the solution above, and measures the materials performance quantitatively.
In SEM analysis, intergranular ashm is clear by the dark lines where the grain boundaries are eaten away.
This abstract is a brief summary of the referenced standard. The bent samples are examined at low magnification, where the appearance of cracks or fissures indicate intergranular attack. Practice A62-13, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date.
Historical Version s – view previous versions of standard.
Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. Each ASTM A Practice ast includes a list of the grades of stainless steels and the acceptable s262-13 structures for the specific alloys. Please share this page: The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes. Because it can be run quickly for screening, we often run this test first.
For example, in highly oxidizing solutions, intergranular attack can a26-13 due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions.
The etch structure types used to classify the specimens are: Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation.
It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels. Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed.
Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard.
Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: The test uses a visual inspection of the surface of the bent specimen to determine pass or fail. The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in use. Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other w262-13 phasessuch as sigma phase, that occurs along the grain boundaries.
A2621-3 is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries. The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.